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This lecture will detail the creation of ultrasensitive sensors based on electronically active conjugated polymers (CPs) and carbon nanotubes (CNTs). A central concept that a single nano- or molecular-wire spanning between two electrodes would create an exceptional sensor if binding of a molecule of interest to it would block all electronic transport. The use of molecular electronic circuits to give signal gain is not limited to electrical transport and CP-based fluorescent sensors can provide ultratrace detection of chemical vapors via amplification resulting from exciton migration. Nanowire networks of CNTs provide for a practical approximation to the single nanowire scheme. These methods include abrasion deposition and selectivity is generated by covalent and/or non-covalent binding selectors/receptors to the carbon nanotubes. Sensors for a variety of materials and cross-reactive sensor arrays will be described. The use of carbon nanotube based gas sensors for the detection of ethylene and other gases relevant to agricultural and food production/storage/transportation are being specifically targeted and can be used to create systems that increase production, manage inventories, and minimize losses.
The utility of carbon nanomaterials is highly dependent upon the precision upon which they can be assembled and functionalized. New methods enable high impact applications in sensing, mechanical, membrane, and energy storage/conversion. Approaches to the formation of functional assemblies of carbon nanotubes will be described that involved the non-covalent immobilization of the materials into functional assemblies. In a non-covalent method, no direct chemical bonds are made to the carbon nanotubes, thereby leaving their electronic properties intact. New covalent connections to the graphene surfaces (sidewalls) of the carbon nanotubes will also be discussed and how these materials can serve to modify their electronic properties for devices as well as hard wire functional assemblies to the carbon nanotubes to provide interactions with chemicals (sensors) or electrocatalysis (energy conversion). Many of these methods are also applicable to the functionalization of graphite to create new forms of graphene. We will also show how high purity graphene can be produced in using new scalable electrochemical methods.